Šestar - baza podataka znanstvenih instrumenata

X-ray single crystal diffractometer Rigaku Synergy S

• Skraćeni naziv instrumenta

  Single crystal X-ray diffractometer

  Inventarni broj

  49050

  Opći opis

  Rigaku XtaLAB Synergy-S is an X-ray diffractometer for X-ray diffraction on a single crystal. It has two PhotonJet-S microfocus sources of X-rays, with anodes made of molybdenum (Mo) and copper (Cu). These third-generation X-ray tubes in combination with microfocus optics represent strong sources of collimated radiation of wavelengths of 0.071 and 0.154 nm. XtaLAB Synergy-S monocrystalline X-ray diffractometer comes with a four-circuit goniometer, in the so-called. kappa configuration, and has a high speed motor for crystal orientation. The system is equipped with a highly sensitive and fast X-ray detector (HyPix-6000HE).
  Very small samples of crystals of small organic molecules and crystals of biological macromolecules such as proteins, less than 10 micrometers in size, can also be measured on this instrument. The diffractometer is equipped with a cryostat that allows the collection of data on samples in the temperature range from 90 to 400 K.

  Uža područja primjene

  crystallography, condensed matter physics, biochemistry

  Namjena instrumenta

  crystal structure determination from organic, inorganic and biological samples

  Popis usluga

  determination of the crystal structure of small molecules; determination of crystal structure of biological macromolecules; determination of charge density; determination of crystal structure under high pressure;

  Opis na stranicama zavoda/laboratorija

  https://www.irb.hr/eng/Research/Capital-equipment/Rendgenski-difraktometar-za-monokristale-Oxford-Diffraction-Xcalibur-Nova-R

  Tijelo koje je financiralo nabavku opreme

  ,

  Project title

  Open scientific infrastructure platforms for innovative applications in the economy and society (O-ZIP)

  Type of instrument

  ,

  Type of the analysis

  , , ,

  Applications

  , , , , , , , , , , ,

  Ključne riječi

  crystallography, protein crystallography, molecule structure, charge density

  Procijenjeni broj korisnika

  50

  Year of manufacture

  2021

• Ustanova en

  Institut Ruđer Bošković
  Bijenička cesta 54, Zagreb

  Zavod

  Department of physical chemistry

  Laboratorij

  Laboratory for chemical and biological crystallography

  Grad

  Zagreb

  Ulica i broj

  Bijenička 54

  Krilo/Kat/Soba

  3. wing, 109

• Način korištenja instrumenta

  , ,

  Cjenik korištenja

  The price per sample is 500kn for users from the RBI and 720kn for external users.

  Popis ovlaštenih korisnika

  Zoran Štefanić
  Krešimir Molčanov
  Aleksandar Višnjevac
  Valentina Milašinović
  Petra Stanić

  Broj istovrsnih instrumenata u ustanovi

  1

• Ime i prezime

  Zoran Štefanić

  Titula

  Dr.

  E-mail

  zoran.stefanic@irb.hr

  Telefon

  01 4571405

  Mobitel

  0912804972

• Ime i prezime

  Krešimir Molčanov

  Titula

  Dr.

  E-mail

  kresimir.molcanov@irb.hr

  Telefon

  4571405

• Model

  Rigaku XtaLAB Synergy-S

  Mrežna (URL) adresa instrumenta na stranicama proizvođača

  https://www.rigaku.com/products/crystallography/synergys

  Princip rada i mjerna tehnika

  An X-ray diffractometer for single crystals illuminates the crystal sample with a beam of X-rays of a fixed wavelength. The structure of the molecules that make up the crystal is determined from a series of diffraction images obtained in various positions of the crystal.
  It is possible to determine the positions of atoms in molecules at the atomic level. The instrument can record data on molecules from just a few atoms to large molecules with tens of thousands of atoms such as proteins.

  Radno i mjerno područje

  positions of atoms on a subnanometar scale, temperature range 90-400K

  Proizvođač

  Rigaku

  Mrežna (URL) adresa proizvođača

  https://rigaku.com

  Purchase price

  2.8

  Estimated current value of equipment

  2.8

  Vijek trajanja

  up to 20 years

  Ostale tehničke karakteristike

  • Four-circle kappa goniometer for high precision crystal positioning and orientation (sphere of confusion less than 10 μm)
  • Equiped with dual wavelength X-ray source with Cu and Mo anodes mounted on the same goniometer
  • Two dimensional, low noise, direct photon counting X-ray detector with fast readout times (in ms) and high dynamic range (at least 24 bits) and no dimension reduction (with eg. optical tapers)
  • Exchangable collimators with apertures 0.2-0.7 mm
  • Safety cabinet with wide opening for easy access to the goniometer, with internal lighting with low heat production
  • Closed circuit, reliable and robust cooling of X-ray tube and detector (air or water)
  • High voltage generator power supply with high voltage and current stability (50 kV, 1mA)
  • Two goniometer heads with possibility of mounting the crystals on glass needles and in cryo loops
  • High intensity microfocs X-ray tubes with focusing of X-rays onto sample crystal and producing low divergence X-ray beam.
  • Liquid nitrogen cryo device capable of maintaining the sample at 100 K with no interruptions. One movable liquid nitrogen vessel of at least 130 L capacity for refilling the system.
  • PC for operating the instrument with software for data acquisition on small molecule and protein samples installed and free upgrades.
  

  Mrežna (URL) adresa s tehničkim karakteristikama

  https://www.rigaku.com/products/crystallography/synergys

  Popratna i dodatna oprema

  Oxford Cryostream 800
  High Pressure Kit

• Slike en
  
  Rigaku XtaLAB Synergy S

  
  Detector and goniometer

  
  Collimators and optics

Natrag en